Analytical Pharmaceutical Chemistry 2

 

 

Analytical Pharmaceutical Chemistry 2

[second semester/second year]

Instructor Information

Instructor

Email

Office Location & Hours

Dr.Fida Am Ali

drfidaamali@gmail.com

[office, 12-14, Monday and wednesday]

General Information

Description

At the end of this course, students are expected to learn

- how to chose the separation method according to chemical structure and physical properties of substance

- Separate the active  substances from pharmaceutical forms

-  apply the separation methods in drug stability studies

- use the separation methods in quality control analyses    

Expectations and Goals

1-          Understanding and all separation techniques

2-          Using separation Instruments in determination the concentration of substances

3-          Using appropriate separation method according to the goal of analysis

4-          Using separation Instruments in the analysis of pharmaceutical preparations as well as the food analyses and the biochemical and clinical analyses.          They are also used in the analysis of contaminants

Language(s) of Instruction: Arabic                                  Textbook(s) Analytical Chemistry (English) and Power point pamphlet (Arabic)

Course Materials

Required Text

[Analytical chemistry] [textbook], [G. Christian]

[Power Point lectures of Analytical Chemistry -2-] [pamphlet], [dr.Fida Am Ali]

 

Course Schedule

 week

 

 

Topic

Reading

Exercises

 

1- 22/9-27/9

Introduction in separation Methods

                   Power Point pamphlet

             Practical session

 

1- 29/9-4/10      

           Extraction Methods                                                                    

                                         Power Point  pamphlet           

   Power                           practical session

 

 

3- 6/10-10/10

          Extraction Methods                                                                                   

                                       Power Point pamphlet  

                          Practical session

 

 

4- 13/10-18/10

       Ion Exchange separation

                      Power Point pamphlet                          

    Practical session

 

 

5- 20/10-25/10

      Principles of      Chromatography

                      Power Point pamphlet                                        

                  Practical session

 

 

6- 27/10-1/11

       Principles of      Chromatography + quiz

                    Power Point pamphlet                                        

                  Practical session

 

 

7- 3/11-8/11

      Thin layer chromatography

                    Power Point pamphlet                                                                    

                   Practical session

 

 

8- 10/11-15/11

      Paper Chromatography

                    Power Point pamphlet                                                                    

                   Practical session

 

 

9- 17/11-22/11

      Column Chromatography

                    Power Point pamphlet                                                                    

                   Practical session

 

 

10- 24/11-29/11

      Gas Chromatography

                    Power Point pamphlet                                                                    

                   Practical session

 

 

11- 1/12-6/12

       Gas Chromatography

                    Power Point pamphlet                                                                    

                   Practical session

 

 

12- 8/12-13/12

       HPLC + quiz

                    Power Point pamphlet                                                                    

                   Practical session

 

 

13- 15/12-20/12

       HPLC

                    Power Point pamphlet                                                                    

                   Practical session

 

 

14- 22/12-27/12

       Electrophoresis

                    Power Point pamphlet                                                                    

                   Practical session

 

 

15- 29/12-3/1

           Capillary Electrophoresis

                    Power Point pamphlet                                                                    

                   Practical session

 

 

                             

 

Testing Schedule

test

Date

   

Reading

Type

language

% of final grade

Quizz 1

27/10-1/11

 

The first 4th subject

written

Arabic

5

Quizz 1

8/12-13/12

 

The subjects from

TLC till HPLC

MCQ

Arabic

5

Final            

6/1-17/1

 

All listed subjects

 MCQ

Arabic

60

 

General notes:

-      Practical session : 30 Marks

 

 

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